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Preparation of nanocrystalline ZrO 2 powder via a chemical route
Septawendar R.a, Sutardi S.a, Purwasasmita B.S.b, Edwin F.a
a Laboratory of Nanomaterials, Department of Advanced Ceramics, Glass, and Enamel, Ministry of Industry of Indonesia, Indonesia
b Laboratory of Material Processing, Engineering Physics Department, Institute of Technology Bandung, Indonesia
[vc_row][vc_column][vc_row_inner][vc_column_inner][vc_separator css=”.vc_custom_1624529070653{padding-top: 30px !important;padding-bottom: 30px !important;}”][/vc_column_inner][/vc_row_inner][vc_row_inner layout=”boxed”][vc_column_inner width=”3/4″ css=”.vc_custom_1624695412187{border-right-width: 1px !important;border-right-color: #dddddd !important;border-right-style: solid !important;border-radius: 1px !important;}”][vc_empty_space][megatron_heading title=”Abstract” size=”size-sm” text_align=”text-left”][vc_column_text]Nanocrystalline ZrO 2 powder was prepared through a chemical route via a reaction between a soluble salt with an organic template in various ratios at a carbonization temperature of 200°C. The homogenization of the nanopowder was assisted by milling the charcoal precursor in a non polar solvent for 24 hours, followed by calcining at 800°C and 1100°C. X-Ray diffraction (XRD) analysis results show that zirconia nanopowder produced has crystallite sizes of about 26-31 nm and 46-50 nm whose major crystal phase is m-ZrO 2 for calcinations at 800 and 1100°C, respectively. Increasing the organic template concentration reduces the particle and crystallite size, while the elevation of the calcination temperature enlarges the particle and crystallite size.[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Author keywords” size=”size-sm” text_align=”text-left”][vc_column_text]Calcination temperature,Chemical routes,Nanocrystallines,Organic templates,ZrO 2[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Indexed keywords” size=”size-sm” text_align=”text-left”][vc_column_text]Calcination temperature,Chemical route,Nanocrystalline,Organic template concentration,ZrO 2[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Funding details” size=”size-sm” text_align=”text-left”][vc_column_text][/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”DOI” size=”size-sm” text_align=”text-left”][vc_column_text][/vc_column_text][/vc_column_inner][vc_column_inner width=”1/4″][vc_column_text]Widget Plumx[/vc_column_text][/vc_column_inner][/vc_row_inner][/vc_column][/vc_row][vc_row][vc_column][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][/vc_column][/vc_row]