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Syntheses of hematite (α-Fe2O3) nanoparticles using microwave-assisted calcination method
Nurhayati T.a, Iskandar F.a, Abdullah M.a, Khairurrijala
a Physics of Electronic Materials Research Division, Faculty of Mathematics and Natural Sciences, Institut Teknologi Bandung, Indonesia
[vc_row][vc_column][vc_row_inner][vc_column_inner][vc_separator css=”.vc_custom_1624529070653{padding-top: 30px !important;padding-bottom: 30px !important;}”][/vc_column_inner][/vc_row_inner][vc_row_inner layout=”boxed”][vc_column_inner width=”3/4″ css=”.vc_custom_1624695412187{border-right-width: 1px !important;border-right-color: #dddddd !important;border-right-style: solid !important;border-radius: 1px !important;}”][vc_empty_space][megatron_heading title=”Abstract” size=”size-sm” text_align=”text-left”][vc_column_text]Hematite (α-Fe2O3) nanoparticles were synthesized from the solution of FeCl3.6H2O and NaOH in water using microwave-assisted calcination method. The syntheses were initially carried out by microwave heating and completed by a calcination process using a simple heating method. The effects of microwave heating time, calcination temperature, and calcination time were investigated. The XRD patterns demonstrated that the obtained nanoparticles are pure hematite. Using the Scherrer method, the average crystallite sizes of hematite nanoparticles were in the range of 35.6 to 54.4 nm. The obtained hematite nanoparticles were spherical with the average particle sizes ranging from 91 to 116 nm as confirmed by the SEM images. © (2013) Trans Tech Publications, Switzerland.[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Author keywords” size=”size-sm” text_align=”text-left”][vc_column_text]Average particle size,Calcination method,Calcination temperature,Calcination time,Heating method,Hematite nanoparticles,Microwave assisted,Scherrer method[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Indexed keywords” size=”size-sm” text_align=”text-left”][vc_column_text]Calcination,Hematite,Microwave heating,Simple heating[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Funding details” size=”size-sm” text_align=”text-left”][vc_column_text][/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”DOI” size=”size-sm” text_align=”text-left”][vc_column_text]https://doi.org/10.4028/www.scientific.net/MSF.737.197[/vc_column_text][/vc_column_inner][vc_column_inner width=”1/4″][vc_column_text]Widget Plumx[/vc_column_text][/vc_column_inner][/vc_row_inner][/vc_column][/vc_row][vc_row][vc_column][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][/vc_column][/vc_row]