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Ionothermal approach for synthesizing AlPO-5 with hexagonal thin-plate morphology influenced by various parameters at ambient pressure
Khoo D.Y.a, Kok W.-M.a, Mukti R.R.b, Mintova S., Ng E.-P.a
a School of Chemical Sciences, Universiti Sains Malaysia, Malaysia
b Division of Inorganic and Physical Chemistry, Institut Teknologi Bandung, Indonesia
c Laboratoire Catalyse and Spectrochimie, ENSICAEN, Université de Caen, France
[vc_row][vc_column][vc_row_inner][vc_column_inner][vc_separator css=”.vc_custom_1624529070653{padding-top: 30px !important;padding-bottom: 30px !important;}”][/vc_column_inner][/vc_row_inner][vc_row_inner layout=”boxed”][vc_column_inner width=”3/4″ css=”.vc_custom_1624695412187{border-right-width: 1px !important;border-right-color: #dddddd !important;border-right-style: solid !important;border-radius: 1px !important;}”][vc_empty_space][megatron_heading title=”Abstract” size=”size-sm” text_align=”text-left”][vc_column_text]Pure and crystalline AlPO-5 with hexagonal thin-plate morphology was synthesized ionothermally in 1-ethyl-2,3-dimethylimidazolium bromide ([edmim]Br) ionic liquid as both the solvent and structure-directing agent (SDA). The resulting microcrystalline solids were characterized using various techniques. Further studies on the influence of chemical compositions and synthesis conditions in the crystallization process of AlPO-5 were also investigated. The results showed that AlPO-5 crystals with hexagonal thin-plate morphology were obtained when [edmim]Br ionic liquid was used in ionothermal treatment. The crystallinity, size and morphology of the AlPO-5 materials were also found to be strongly influenced by two major factors, chemical composition of the gel mixture and the heating time of the gel mixture. © 2013 Elsevier Masson SAS. All rights reserved.[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Author keywords” size=”size-sm” text_align=”text-left”][vc_column_text]AlPO-5,Aluminophosphates,Chemical compositions,Crystallization process,Ionothermal synthesis,Microcrystalline solids,Structure directing agents,Thin plate[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Indexed keywords” size=”size-sm” text_align=”text-left”][vc_column_text]AlPO-5,Aluminophosphate,Ionic liquid,Ionothermal synthesis,Thin plate[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”Funding details” size=”size-sm” text_align=”text-left”][vc_column_text]The authors are thankful for the financial supports received from Universiti Sains Malaysia through the USM Short-Term Grant ( 304/PKIMIA/6310084 ), RU-PGRS Grant ( 101/PKIMIA/835009 ) and COMSTECH-TWAS Research Grants.[/vc_column_text][vc_empty_space][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][vc_empty_space][megatron_heading title=”DOI” size=”size-sm” text_align=”text-left”][vc_column_text]https://doi.org/10.1016/j.solidstatesciences.2013.08.008[/vc_column_text][/vc_column_inner][vc_column_inner width=”1/4″][vc_column_text]Widget Plumx[/vc_column_text][/vc_column_inner][/vc_row_inner][/vc_column][/vc_row][vc_row][vc_column][vc_separator css=”.vc_custom_1624528584150{padding-top: 25px !important;padding-bottom: 25px !important;}”][/vc_column][/vc_row]